NMR Studies of Phakellins and Isophakellins


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Matthias.Koeck [ at ] awi.de

Abstract

Phakellins 3 and 4 and isophakellins 5 and 6 are tetracyclic pyrrole-imidazole alkaloids. Their structure elucidation is herein reviewed using state-of-the-art NMR methods. Special emphasis has been given to the application of ADEQUATE NMR pulse sequences. Furthermore, 15N NMR chemical shifts, proton T1 relaxation times, and 1J CH coupling constants were determined. © 2008 American Chemical Society and American Society of Pharmacognosy.



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Published
Eprint ID
19160
DOI https://www.doi.org/10.1021/np8000706

Cite as
Meyer, S. W. and Köck, M. (2008): NMR Studies of Phakellins and Isophakellins , Journal of Natural Products, 71 (9), pp. 1524-1529 . doi: https://www.doi.org/10.1021/np8000706


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