Pectenotoxins and yessotoxin from Arica Bay, North Chile as determined by tandem mass spectrometry


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Bernd.Krock [ at ] awi.de

Abstract

Lipophilic phycotoxins were measured by tandem mass spectrometry coupled to liquid chromatography (LC-MS/MS) in size-fractionated plankton samples taken at five stations in Arica Bay, northern Chile in the southern summer 2007/2008. Pectenotoxins-2 (PTX-2), -11 (PTX-11), -2 seco acid (PTX-2sa) and yessotoxin (YTX) were identified by comparison of retention times and collision-induced mass spectra of certified standards and field sample extracts. This is the first report of PTXs and YTX from planktonic samples in Chilean coastal waters. © 2009 Elsevier Ltd. All rights reserved.



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Eprint ID
20372
DOI https://www.doi.org/10.1016/j.toxicon.2009.04.013

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Krock, B. , Seguel, C. G. , Valderrama, K. and Tillmann, U. (2009): Pectenotoxins and yessotoxin from Arica Bay, North Chile as determined by tandem mass spectrometry , Toxicon, 54 (3), pp. 364-367 . doi: https://www.doi.org/10.1016/j.toxicon.2009.04.013


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